1,1,2,3-四氯-1-氟丙烷合成路线 (共 4 条)
反应条件
antimony(V) pentachloride; SbF3
参考文献
Nesmeyanov,A.N. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1960 , p. 415 - 419
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1960 , p. 447 - 451
反应条件
hydrogen fluoride
T=290°C; P=750.075 Torr; 3 h; Inert atmospheretubular reactor;
参考文献
Nose, Masatoshi; Yamashita, Tsuneo; Suzuki, Atsushi
Patent: US2012/65434 A1, 2012 ;
Location in patent: Page/Page column 5 ;
反应条件
hydrogen fluoride
T=290°C; 3 h; HASTELLOY.(R). tubular reactorInert atmosphere; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.; NOSE, Masatoshi; YAMASHITA, Tsuneo; SUZUKI, Atsushi
Patent: WO2010/131766 A2, 2010 ;
Location in patent: Page/Page column 13-15 ;
反应条件
hydrogen fluoride
T=110°C; P=13689.1 - 17567.8 Torr; 9.5 h; Product distribution / selectivity;
参考文献
Merkel, Daniel C.; Tung, Hsueh Sung; Pokrovski, Konstantin A.; Wang, Haiyou; Bektesevic, Selma
Patent: US2012/178977 A1, 2012 ;
Location in patent: Page/Page column 5 ;