2-甲基-1-(三甲基硅杂氧基)-1-丙烯合成路线 （共 23 条）
反应条件
1: With anhydrous lithium acetate in N,N-dimethyl-formamide
T=20°C; 16 h;
2: With hydrogenchloride in N,N-dimethyl-formamide
T=-45°C;
3: With sodium tetrahydroborate; sodium hydrogencarbonate in methanol; N,N-dimethyl-formamide
T=-45 - 20°C;
参考文献
Kawano, Yoshikazu; Fujisawa, Hidehiko; Mukaiyama, Teruaki
Chemistry Letters, 2005 , vol. 34, # 4 p. 614 - 615
反应条件
triphenylemethane; methyllithium in ethylene glycol dimethyl ether
参考文献
Stang,P.J. et al.
Journal of the American Chemical Society, 1974 , vol. 96, p. 4562 - 4569
反应条件
1: TMSO-CH=C(Me)2 With nonafluoro-n-butanesulfonyl fluoride; tetrabutyl ammonium fluoride in tetrahydrofuran
T=20°C; 16 h;
2: acrylic acid methyl ester With palladium diacetate; tetrabutyl-ammonium chloride; potassium carbonate in N,N-dimethyl-formamide
T=25°C; 6 h;
参考文献
Lyapkalo, Ilya M.; Webel, Matthias; Reissig, Hans-Ulrich
European Journal of Organic Chemistry, 2002 , # 21 p. 3646 - 3658
