1,2,3,4-四氢-6-甲基喹噁啉合成路线 （共 5 条）
反应条件
C21H21ClIrNO2 in tetrahydrofuran; 2,2,2-trifluoroethanol 20 h; Inert atmosphere;
参考文献
Wu, Jianjun; Talwar, Dinesh; Johnston, Steven; Yan, Ming; Xiao, Jianliang
Angewandte Chemie - International Edition, 2013 , vol. 52, # 27 p. 6983 - 6987
Ross. Khim. Zh., 2013 , vol. 125, # 27 p. 7121 - 7125,5
反应条件
C26H29ClIrNO3; hydrogen in 2,2,2-trifluoroethanol
T=20°C; P=760.051 Torr; 3 h;
参考文献
Wu, Jianjun; Barnard, Jonathan H.; Zhang, Yi; Talwar, Dinesh; Robertson, Craig M.; Xiao, Jianliang
Chemical Communications, 2013 , vol. 49, # 63 p. 7052 - 7054
反应条件
hydrogenchloride; sodium chloride in methanol; sodium borohydride
参考文献
Maxia Pharmaceuticals, Inc.
Patent: US6515003 B1, 2003 ;
反应条件
1: sodium acetate; aqueous acetic acid
2: platinum; benzene / 2206.5 - 4413.05 Torr / Hydrogenation
View Scheme
参考文献
Cavagnol; Wiselogle
Journal of the American Chemical Society, 1947 , vol. 69, p. 795,796
反应条件
1: Raney nickel; benzene / Hydrogenation
2: sodium acetate; aqueous acetic acid
3: platinum; benzene / 2206.5 - 4413.05 Torr / Hydrogenation
View Scheme
参考文献
Cavagnol; Wiselogle
Journal of the American Chemical Society, 1947 , vol. 69, p. 795,796
