3,5-二甲氧基-4-羟基甲苯合成路线 (共 38 条)
反应条件
hydrogen; sodium sulfate; Co(II, III) tetrachlorocatechol catalyst T=320 - 345°C; P=2311.54 Torr; 2.25 h; Sealed reactor;
参考文献
US2012/123171 A1, ;
Page/Page column 3 ;
反应条件
pyridine; sodium methylate; sodium; Copper(I)chloride in methanol; toluene
反应条件
lithium aluminium tetrahydride in tetrahydrofuran; chlorobenzene 2 h; Heating;
参考文献
Baik, Woonphil; Lee, Hyun Joo; Koo, Sangho; Kim, Byeong Hyo
Tetrahedron Letters, 1998 , vol. 39, # 44 p. 8125 - 8128
参考文献
Chemische Berichte, , vol. 85, p. 1181,1188
反应条件
copper(I) bromide in water; N,N-dimethyl-formamide
参考文献
Tetrahedron Letters, , vol. 46, # 8 p. 1255 - 1257
反应条件
1: LiAlH4 / tetrahydrofuran 2: H2 / Pd-C 3: aq. NaOH / 120 °C View Scheme
参考文献
Acta Chemica Scandinavica (1947-1973), , vol. 27, p. 1355 - 1368
反应条件
1: K2CO3 / dimethylsulfoxide 2: LiAlH4 / tetrahydrofuran 3: H2 / Pd-C 4: aq. NaOH / 120 °C View Scheme
参考文献
Acta Chemica Scandinavica (1947-1973), , vol. 27, p. 1355 - 1368
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Justus Liebigs Annalen der Chemie, , vol. 763, p. 109 - 120
反应条件
1: HCl 2: LiAlH4 / tetrahydrofuran View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 763, p. 109 - 120