2-氨基-3-硝基-4-甲基吡啶合成路线 （共 22 条）
反应条件
sulfuric acid; nitric acid T=0 - 70°C; 4 h;
参考文献
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, , vol. 96, p. 952 - 962
反应条件
1: With sulfuric acid; nitric acid T=0 - 50°C; 24 h; 2: in water pH=7; Cooling with ice;
参考文献
EP2366691 A1, ;
Page/Page column 6-7 ;
反应条件
in methanol 0.416667 h; Irradiation;
参考文献
Acta Chimica Hungarica, , vol. 121, # 4 p. 333 - 338
反应条件
in acetic acid 5 h; Heating;
参考文献
Archiv der Pharmazie, , vol. 326, # 4 p. 199 - 202
反应条件
sulfuric acid T=75°C; 2 h; other pyridine nitramines, var. acid concentrations, var. temp., var. time; Mechanism;
参考文献
Australian Journal of Chemistry, , vol. 36, # 6 p. 1159 - 1166
参考文献
Chemische Berichte, , vol. 57, p. 794
反应条件
2: phosphoryl chloride 3: acetic acid; sodium acetate; palladium/charcoal / Hydrogenation 4: ethyl nitrite; petroleum ether / Diazotization 5: KMnO4; H2O View Scheme
参考文献
Roe; Seligman
Journal of Organic Chemistry, 1955 , vol. 20, p. 1729,1731
反应条件
nitric acid in conc. H2 SO4
参考文献
Merck and Co., Inc.
Patent: US5412097 A1, 1995 ;
US 5412097 A
反应条件
hydrazine in water T=110 - 120°C; 5 h;
参考文献
Smolyar; Yutilov
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 1 p. 115 - 118
反应条件
2: phosphoryl chloride 3: acetic acid; sodium acetate; palladium/charcoal / Hydrogenation 4: ethyl nitrite; petroleum ether / Diazotization View Scheme
参考文献
Roe; Seligman
Journal of Organic Chemistry, 1955 , vol. 20, p. 1729,1731
