(S)-2-(1-甲氧基-1-甲基乙氧基)-丁二醇合成路线 （共 6 条）
反应条件
2: 83.8 percent / K2CO3 / methanol / 18 h / 23 °C View Scheme
参考文献
Meyers; Lawson; Walker; Linderman
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5111 - 5123
反应条件
boron trifluoride diethyl etherate in diethyl ether 3 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Meyers; Lawson; Walker; Linderman
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5111 - 5123
反应条件
1: BF3*Et2O / diethyl ether / 3 h / Ambient temperature 2: 48.3 percent / CrO3 / pyridine; CH2Cl2 / 1.) 0 deg C, 20 min, 2.) 23 deg C, 20 min View Scheme
参考文献
Meyers; Lawson; Walker; Linderman
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5111 - 5123
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
5 h; Ambient temperature;
参考文献
Meyers; Lawson; Walker; Linderman
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5111 - 5123
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=50°C; 8-12h;
参考文献
Boger, Dale L.; Panek, James S.
Journal of Organic Chemistry, 1981 , vol. 46, # 6 p. 1208 - 1210
反应条件
boron trifluoride diethyl etherate in diethyl ether
3 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Meyers; Lawson; Walker; Linderman
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5111 - 5123
