3,5-二氨基-4-甲基苯甲酸合成路线 （共 7 条）
反应条件
durch Austausch von NH2 gegen Cl;
参考文献
Claus; Beysen
Justus Liebigs Annalen der Chemie, 1891 , vol. 266, p. 223,227
反应条件
hydrogenchloride; tin
参考文献
Marckwald
Justus Liebigs Annalen der Chemie, 1893 , vol. 274, p. 357
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Claus; Joachim
Justus Liebigs Annalen der Chemie, 1891 , vol. 266, p. 218
反应条件
1: HNO3+H2SO4
2: tin; hydrochloric acid
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参考文献
Claus; Joachim
Justus Liebigs Annalen der Chemie, 1891 , vol. 266, p. 218
反应条件
1: 89 percent / H2SO4 / Heating
2: 78 percent / Na2CO3 / acetone / Heating
3: 78 percent / aq. NaOH / tetrahydrofuran / Heating
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参考文献
Ziessel, Raymond; Pickaert, Guillaume; Camerel, Franck; Donnio, Bertrand; Guillon, Daniel; Cesario, Michele; Prange, Thierry
Journal of the American Chemical Society, 2004 , vol. 126, # 39 p. 12403 - 12413
参考文献
Kauffmann; Weissel
Justus Liebigs Annalen der Chemie, 1912 , vol. 393, p. 25
反应条件
1: 89 percent / H2SO4 / Heating
2: 72 percent / Na2CO3 / acetone / Heating
3: 74 percent / aq. NaOH / tetrahydrofuran / Heating
View Scheme
参考文献
Ziessel, Raymond; Pickaert, Guillaume; Camerel, Franck; Donnio, Bertrand; Guillon, Daniel; Cesario, Michele; Prange, Thierry
Journal of the American Chemical Society, 2004 , vol. 126, # 39 p. 12403 - 12413
反应条件
1: 89 percent / H2SO4 / Heating
2: 78 percent / Na2CO3 / acetone / Heating
3: 72 percent / aq. NaOH / tetrahydrofuran / Heating
View Scheme
参考文献
Ziessel, Raymond; Pickaert, Guillaume; Camerel, Franck; Donnio, Bertrand; Guillon, Daniel; Cesario, Michele; Prange, Thierry
Journal of the American Chemical Society, 2004 , vol. 126, # 39 p. 12403 - 12413
