1,3-二甲基-6-亚氨基-5-异亚硝基尿嘧啶合成路线 （共 29 条）
反应条件
acetic acid; sodium nitrite in water
参考文献
LIFE and BRAIN GMBH; MUeLLER, Christa; ZIMMER, Andreas; LABS, Stefanie; BUCHHOLZ, Stephanie; HINZ, Sonja
Patent: WO2012/76974 A1, 2012 ;
Location in patent: Page/Page column 27; 29 ;
反应条件
sodium nitrite in water T=50°C;
参考文献
Shirsagar; Bhave
Journal of the Indian Chemical Society, 1997 , vol. 74, # 8 p. 649 - 651
参考文献
DE206453 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 9, p. 1005
反应条件
1: aq. NaOH solution 2: aqueous acetic acid; NaNO2 View Scheme
参考文献
Zhurnal Obshchei Khimii, , vol. 16, p. 179,183
Chem.Abstr., , p. 96
反应条件
1: aq. NaOH solution; NaOH 2: aq. NaOH solution 3: aqueous acetic acid; NaNO2 View Scheme
参考文献
Zhurnal Obshchei Khimii, , vol. 16, p. 179,183
Chem.Abstr., , p. 96
反应条件
1: With acetic anhydride 2:
参考文献
Polyhedron, , vol. 50, # 1 p. 10 - 15
反应条件
sodium dithionite; ammonia in water T=70 - 80°C; 0.25 h;
参考文献
LIFE and BRAIN GMBH; MUeLLER, Christa; ZIMMER, Andreas; LABS, Stefanie; BUCHHOLZ, Stephanie; HINZ, Sonja
Patent: WO2012/76974 A1, 2012 ;
Location in patent: Page/Page column 27; 30 ;
反应条件
in water cyclic voltametry, pH=7; Mechanism;
参考文献
Avrutskaya, Inna; Fioshin, Michail
Collection of Czechoslovak Chemical Communications, 1982 , vol. 47, # 1 p. 196 - 202
反应条件
1: 90 percent / tetrahydrofuran / 12 h / Ambient temperature 2: 79 percent / tetrahydrofuran / 12 h / Ambient temperature View Scheme
参考文献
Igarashi, Mamoru; Tada, Masaru
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 3 p. 807 - 810
参考文献
Dick et al.
Journal of the Chemical Society, 1956 , p. 2131,2135
