2,2,3,3-四氟丙酰氯合成路线 (共 3 条)
反应条件
α,α,α-trichlorotoluene T=50 - 75°C;
参考文献
Schwertfeger, W.; Siegemund, G.
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 237 - 246
参考文献
Journal of the American Chemical Society, , vol. 80, p. 6442,6443
反应条件
magnesium diethoxide in benzene 1.) 10-15 deg C, 1 h, 2.) ca.20 deg C, 3 h, 3.) overnight;
参考文献
Krokhalev, V. M.; Saloutin, V. I.; Pashkevich, K. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 10 p. 2099 - 2104
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 10 p. 2266 - 2272