反应条件
1.1: CuBr; NaNO2; HBr / H2O / 1 h / 10 - 15 °C 1.2: 67 percent / CuBr; HBr / H2O / 0.17 h / Heating 2.1: t-BuLi / tetrahydrofuran; hexane / 0.33 h / -78 °C 2.2: B(OCH3)3 / tetrahydrofuran; hexane / 2 h / -78 °C 2.3: 82 percent / peracetic acid / tetrahydrofuran; acetic acid; H2O / 1 h / -10 °C View Scheme
参考文献
Holladay, Mark W.; Bai, Hao; Li, Yihong; Lin, Nan-Horng; Daanen, Jerome F.; Ryther, Keith B.; Wasicak, James T.; Kincaid, John F.; He, Yun; Hettinger, Anne-Marie; Huang, Peggy; Anderson, David J.; Bannon, Anthony W.; Buckley, Michael J.; Campbell, Jeffrey E.; Donnelly-Roberts, Diana L.; Gunther, Karen L.; Kim, David J. B.; Kuntzweiler, Theresa A.; Sullivan, James P.; Decker, Michael W.; Arneric, Stephen P.
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 19 p. 2797 - 2802
