2-烯丙基-4-甲基苯酚合成路线 （共 41 条）
反应条件
Product distribution;
参考文献
Claisen
Justus Liebigs Annalen der Chemie, 1925 , vol. 442, p. 227
Journal fuer Praktische Chemie (Leipzig), 1922 , vol. <2> 105, p. 66
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Claisen
Patent: DE412169 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 15, p. 268
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Claisen
Angewandte Chemie, 1923 , vol. 36, p. 478
Justus Liebigs Annalen der Chemie, 1925 , vol. 442, p. 244
参考文献
Claisen
Justus Liebigs Annalen der Chemie, 1925 , vol. 442, p. 227
Journal fuer Praktische Chemie (Leipzig), 1922 , vol. <2> 105, p. 66
反应条件
1: 85 percent / aq. NaOH; tetrabutylammonium bromide / 4 h / Heating
2: 90 percent / KO-t-Bu / tetrahydrofuran / 0.5 h / Heating
3: 88 percent / Grubbs catalyst / CH2Cl2 / 8 h / 20 °C
View Scheme
参考文献
Tsai, Tzu-Wei; Wang, Eng-Chi; Li, Sie-Rong; Chen, Yung-Hua; Lin, Yu-Li; Wang, You-Feng; Huang, Keng-Shiang
Journal of the Chinese Chemical Society, 2004 , vol. 51, # 6 p. 1307 - 1318
反应条件
tin(IV) chloride in dichloromethane
Ambient temperature;
参考文献
Attanasi, Orazio A.; Filippone, Paolino; Balducci, Sandro
Gazzetta Chimica Italiana, 1991 , vol. 121, # 10 p. 487 - 489
参考文献
Claisen; Eisleb
Justus Liebigs Annalen der Chemie, 1913 , vol. 401, p. 44
反应条件
sodium hydroxide in water
T=100°C; 4 h;
参考文献
Achari; Bandyopadhyay; Basu; Pakrashi
Tetrahedron, 1985 , vol. 41, # 1 p. 107 - 110
反应条件
diethyl benzenedicarboxylate; sulfur
T=240°C;
参考文献
Mollier; Lozac'h
Bulletin de la Societe Chimique de France, 1958 , p. 651,655
反应条件
1: 84 percent / NaOH / H2O / 4 h / 100 °C
2: 1.) Hg(OAc)2; 2.) NaBH4 / 1.) aq. THF, r.t., 20 min; 2.) 3M NaOH
3: 87 percent / Na2Cr2O7, conc H2SO4 / dimethylsulfoxide / 0.75 h / 70 °C
View Scheme
参考文献
Achari; Bandyopadhyay; Basu; Pakrashi
Tetrahedron, 1985 , vol. 41, # 1 p. 107 - 110
反应条件
1: platinum; ethanol / Hydrogenation
2: aqueous NaOH; acetone / 0 °C
3: 250 °C
4: platinum; methanol / Hydrogenation
5: ethanolic NaOH
View Scheme
参考文献
Hurd; Yarnall
Journal of the American Chemical Society, 1937 , vol. 59, p. 1686,1688
反应条件
ethanol; platinum
Hydrogenation;
参考文献
Hurd; Yarnall
Journal of the American Chemical Society, 1937 , vol. 59, p. 1686,1688
