4-烯丙基-2,6-二甲氧基苯酚合成路线 (共 49 条)
反应条件
T=150°C; Claisen rearrangement; 336000 h;
参考文献
Rudroff, Florian; Rydz, Joanna; Ogink, Freek H.; Fink, Michael; Mihovilovic, Marko D.
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 8-9 p. 1436 - 1444
反应条件
1: 81 percent / ZnCl2 / propionic acid / Heating 2: 98 percent / K2CO3 View Scheme
参考文献
Journal of the Chinese Chemical Society, , vol. 51, # 5 A p. 1001 - 1004
反应条件
1: 98 percent / K2CO3 View Scheme
参考文献
Journal of the Chinese Chemical Society, , vol. 51, # 5 A p. 1001 - 1004
反应条件
sodium tetrahydroborate in methanol; benzene Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 50, # 7 p. 941 - 945
反应条件
sodium hydroxide T=70 - 80°C; 2 h;
参考文献
Synthetic Communications, , vol. 26, # 13 p. 2569 - 2572
反应条件
in 1,3,5-trimethyl-benzene T=160 - 165°C; 2.5 h;
参考文献
Chemistry Letters, , p. 625 - 626
参考文献
Li, Guoqing; Li, Zhan; Fang, Xiuhua
Synthetic Communications, 1996 , vol. 26, # 13 p. 2569 - 2572
反应条件
1: 4.1 g / CH3COONa / benzene / 0.58 h 2: 1.) aq. NaHCO3, 2.)NaBH4 View Scheme
参考文献
Tetrahedron Letters, , vol. 23, # 37 p. 3815 - 3818
反应条件
1: 36.6 percent / aq. NaOH / 2 h / 70 - 80 °C 2: 48.6 percent / 2 h / 200 °C View Scheme
参考文献
Synthetic Communications, , vol. 26, # 13 p. 2569 - 2572
反应条件
1: 86 percent / H2SO4 / 50 h / Ambient temperature 2: 40 percent / aq. NaOH / 2 h / 70 - 80 °C View Scheme
参考文献
Synthetic Communications, , vol. 26, # 13 p. 2569 - 2572