4-环戊-2-烯-1-基苯酚合成路线 (共 14 条)
反应条件
1: 90.6 percent / PdCl2(PhCN)2 / benzene / 2 h / Heating 2: 91.6 percent / 30percent H2O2, conc. HCl / acetonitrile / 3 h / 50 °C / the excess of H2O2 was removed by catalytic hydrogenation using 10percent Pd-C View Scheme
参考文献
Rao, Darvasula V.; Stuber, Fred A.
Tetrahedron Letters, 1981 , vol. 22, # 25 p. 2337 - 2340
反应条件
1: 90.6 percent / PdCl2(PhCN)2 / benzene / 2 h / Heating 2: 30percent H2O2, conc. HCl / acetonitrile / 3 h / 50 °C / the excess of H2O2 was removed by catalytic hydrogenation using 10percent Pd-C View Scheme
参考文献
Rao, Darvasula V.; Stuber, Fred A.
Tetrahedron Letters, 1981 , vol. 22, # 25 p. 2337 - 2340
反应条件
methanol; platinum Hydrogenation;
参考文献
Bader
Journal of the American Chemical Society, 1953 , vol. 75, p. 5967
反应条件
1: phenol With phosphoric acid in water; toluene
T=20°C; 2 h;
2: cyclopenta-1,3-diene in water; toluene
T=20°C; 4 h;
参考文献
Fullam, Elizabeth; Abuhammad, Areej; Wilson, David L.; Anderton, Matthew C.; Davies, Steve G.; Russell, Angela J.; Sim, Edith
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 4 p. 1185 - 1190
反应条件
lignosulfonic acids in para-xylene
T=140°C; Alkylation; 1 h;
参考文献
Pisanenko; Smirnov-Zamkov
Russian Journal of Applied Chemistry, 1999 , vol. 72, # 9 p. 1655 - 1657
反应条件
phosphoric acid
4 h; Ambient temperature;
参考文献
Rao, Darvasula V.; Stuber, Fred A.
Tetrahedron Letters, 1981 , vol. 22, # 25 p. 2337 - 2340
反应条件
phosphoric acid
4 h; Ambient temperature;
参考文献
Rao, Darvasula V.; Stuber, Fred A.
Tetrahedron Letters, 1981 , vol. 22, # 25 p. 2337 - 2340
反应条件
1: 200 - 280 °C
2: 85percent H3PO4 / toluene / 2 h / Ambient temperature
View Scheme
参考文献
Dai, S. H.; Lin, C. Y.; Rao, D. V.; Stuber, F. A.; Carleton, P. S.; Ulrich, Henri
Journal of Organic Chemistry, 1985 , vol. 50, # 10 p. 1722 - 1725
参考文献
Bader
Journal of the American Chemical Society, 1953 , vol. 75, p. 5967
反应条件
potassium carbonate
48 h; Heating;
参考文献
Kumar, Surat; Rastogi, Shri Nivas
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 7 p. 659 - 663