2,2,2-三甲基乙酰苯胺合成路线 (共 72 条)
反应条件
triethylamine in dichloromethane T=0 - 20°C;
参考文献
Shi, Feng; Li, Jian; Li, Chunju; Jia, Xueshun
Tetrahedron Letters, 2010 , vol. 51, # 46 p. 6049 - 6051
反应条件
diphosphorous tetraiodide in tetrachloromethane; dichloromethane Heating;
参考文献
Suzuki, Hitomi; Tsuji, Junko; Sato, Naofumi; Osuka, Atsuhiro
Chemistry Letters, 1983 , p. 449 - 452
反应条件
tert-butylisonitrile in dichloromethane T=20°C; 2 h;
参考文献
Rao, Yu; Li, Xuechen; Danishefsky, Samuel J.
Journal of the American Chemical Society, 2009 , vol. 131, # 36 p. 12924 - 12926
反应条件
hydrogenchloride; acetic acid
参考文献
Chemische Berichte, , vol. 44, p. 1202
反应条件
in tetrahydrofuran T=40°C; 3 h;
参考文献
Krishnamurthy, S.
Tetrahedron Letters, 1982 , vol. 23, # 33 p. 3315 - 3318
反应条件
N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide T=25°C; 16 h;
参考文献
Sasaki, Kaname; Crich, David
Organic Letters, 2011 , vol. 13, # 9 p. 2256 - 2259
反应条件
trifluorormethanesulfonic acid; tris(4-methylphenyl)-phosphine; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in 1,2-dichloro-ethane Beckmann rearrangement; 3 h; Heating;
参考文献
Organic Letters, , vol. 3, # 2 p. 311 - 312
反应条件
1: in tetrahydrofuran T=-78 - 0°C; 2: With water in tetrahydrofuran
参考文献
Barluenga, Jose; Fananas, Francisco J.; Sanz, Roberto; Marcos, Cesar; Ignacio, Jose M.
Chemical Communications, 2005 , # 7 p. 933 - 935
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2 in 2-cyclohexylethanol T=130°C; 15 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 130, # 47 p. 15982 - 15989
反应条件
hydroxylamine hydrochloride; trifluoroacetic acid T=70°C; Beckmann Rearrangement; 16 h; Inert atmosphere;
参考文献
Catalysis Communications, , vol. 49, p. 47 - 51