4-(1-甲基-1-苯基-乙基)-苯甲醚合成路线 (共 12 条)
参考文献
Welsh; Drake
Journal of the American Chemical Society, 1938 , vol. 60, p. 59,61
反应条件
calcium triflimide; nBu4NPF6 in dichloromethane
T=20°C; 0.5 h;
参考文献
Niggemann, Meike; Bisek, Nicola
Chemistry - A European Journal, 2010 , vol. 16, # 37 p. 11246 - 11249
反应条件
[Fe(III)(TPP)]SbF6 in 1,2-dichloro-ethane
T=80°C; Friedel-Crafts Alkylation; 5 h; Sealed tubeInert atmosphere; Overall yield = 28 percent; regioselective reaction;
参考文献
Teranishi, Satoru; Kurahashi, Takuya; Matsubara, Seijiro
Synlett, 2013 , vol. 24, # 16 art. no. ST-2013-U0620-L, p. 2148 - 2152
反应条件
phosphoric acid
T=90°C;
参考文献
Van Walree, Cornelis A.; Roest, Martin R.; Schuddeboom, Wouter; Jenneskens, Leonardus W.; Verhoeven, Jan W.; Warman, John M.; Kooijman, Huub; Spek, Anthony L.
Journal of the American Chemical Society, 1996 , vol. 118, # 35 p. 8395 - 8407
反应条件
titanium tetrachloride
T=80°C; Alkylation; 4 h;
参考文献
Liguori, Lucia; Bjorsvik, Hans-Rene; Fontana, Francesca; Bosco, Dino; Galimberti, Laura; Minisci, Francesco
Journal of Organic Chemistry, 1999 , vol. 64, # 24 p. 8812 - 8815
反应条件
1: methoxybenzene With 3,4,5,6-tetrachloro-1,2-benzoquinone; [CpMoCl(CO)3]
T=20°C; Friedel Crafts-type alkylation; 0.5 h; Inert atmosphere;
2: isopropenylbenzene T=150°C; Friedel Crafts-type alkylation; 1 h; Inert atmospheresealed tubeMicrowave irradiation;
参考文献
Yamamoto, Yoshihiko; Itonaga, Kouhei
Chemistry - A European Journal, 2008 , vol. 14, # 34 p. 10705 - 10715
参考文献
Welsh; Drake
Journal of the American Chemical Society, 1938 , vol. 60, p. 59,61
参考文献
Welsh; Drake
Journal of the American Chemical Society, 1938 , vol. 60, p. 59,61
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Granoth,I. et al.
Journal of Organic Chemistry, 1976 , vol. 41, # 23 p. 3682 - 3687
反应条件
1: Na
2: AlCl3, HCl
View Scheme
参考文献
Kovacic,P.; Kurz,M.E.
Journal of Organic Chemistry, 1966 , vol. 31, p. 2459 - 2467