1,2,3,4-四-O-乙酰基-6-O-对甲苯磺酰基-beta-D-吡喃葡萄糖合成路线 （共 9 条）
反应条件
acetic acid
Behandeln mit Acetanhydrid und Pyridin;
参考文献
Ohle; v. Vargha
Chemische Berichte, 1929 , vol. 62, p. 2425,2433
Chemische Berichte, 1928 , vol. 61, p. 1208,1210
Full Text Show Details
Compton
Journal of the American Chemical Society, 1938 , vol. 60, p. 395,398
反应条件
1: D-glucopyranose; p-toluenesulfonyl chloride With pyridine
T=0°C; 20 h;
2: acetic anhydride T=0 - 20°C; 1 h;
参考文献
Maschauer, Simone; Haubner, Roland; Kuwert, Torsten; Prante, Olaf
Molecular Pharmaceutics, 2014 , vol. 11, # 2 p. 505 - 515
反应条件
1: D-glucose; p-toluenesulfonyl chloride With pyridine
T=20°C; 12 h;
2: acetic anhydride T=20°C;
参考文献
Budesinsky, Milos; Polakova, Jana; Hamernikova, Michaela; Cisarova, Ivana; Trnka, Tomas; Cerny, Miloslav
Collection of Czechoslovak Chemical Communications, 2006 , vol. 71, # 3 p. 311 - 336
反应条件
pyridine
anschliessend Behandeln mit Acetanhydrid;
参考文献
Hardegger; Montavon
Helvetica Chimica Acta, 1946 , vol. 29, p. 1199,1203
Full Text Show Details
Stanek; Tajmr
Collection of Czechoslovak Chemical Communications, 1959 , vol. 24, p. 1013,1015
反应条件
1: hydrogen bromide; acetic acid
2: pyridine
View Scheme
参考文献
Helferich; Klein
Justus Liebigs Annalen der Chemie, 1926 , vol. 450, p. 219,228
Justus Liebigs Annalen der Chemie, 1927 , vol. 455, p. 173,178
参考文献
Helferich; Klein
Justus Liebigs Annalen der Chemie, 1926 , vol. 450, p. 219,228
Justus Liebigs Annalen der Chemie, 1927 , vol. 455, p. 173,178
反应条件
pyridine
1.) RT, 3 d, 2.) 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Contour-Galcera, Marie-Odile; Guillot, Jean-Michel; Ortiz-Mellet, Carmen; Pflieger-Carrara, Francoise; Defaye, Jacques; Gelas, Jacques
Carbohydrate Research, 1996 , vol. 281, # 1 p. 99 - 118
参考文献
Korytnyk; Mills
Journal of the Chemical Society, 1959 , p. 636,644
反应条件
acetic anhydride; sodium iodide
参考文献
Garrido Espinosa
An. Univ. catol. Valparaiso, 1957 , # 4 p. 245,249
