trichloromethyl silane; sodium iodide in acetonitrile Hydrolysis;

1: 85 percent / NaH / benzene / 4 h / 80 °C 2: 100 percent Chromat. / NaBH4 / methanol / 4 h 3: pTsOH*H2O / benzene / 4 h / Heating 4: trichloromethylsilane; NaI / acetonitrile View Scheme

1: 100 percent Chromat. / NaBH4 / methanol / 4 h 2: pTsOH*H2O / benzene / 4 h / Heating 3: trichloromethylsilane; NaI / acetonitrile View Scheme

1: pTsOH*H2O / benzene / 4 h / Heating 2: trichloromethylsilane; NaI / acetonitrile View Scheme