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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
66122-70-1
合成路线
(共 20 条)
26164-07-8
→
反应条件
66122-70-1
反应条件
jones reagent in acetic acid T=0°C; 0.5 h;
参考文献
Antus, Sandor; Snatzke, Guenther; Steinke, Iris
Liebigs Annalen der Chemie, 1983 , # 12 p. 2247 - 2261
61436-73-5
2-烯炳基苯甲酸
→
反应条件
66122-70-1
反应条件
copper(II) bis(trifluoromethanesulfonate); triphenylphosphine; ruthenium trichloride; silver trifluoromethanesulfonate in acetonitrile T=80°C; 96 h;
参考文献
Ohta, Tetsuo; Kataoka, Yohei; Miyoshi, Akio; Oe, Yohei; Furukawa, Isao; Ito, Yoshihiko
Journal of Organometallic Chemistry, 2007 , vol. 692, # 1-3 p. 671 - 677
118-90-1
邻甲基苯甲酸
+
75-07-0
乙醛
→
反应条件
66122-70-1
反应条件
1: ortho-methylbenzoic acid With sec.-butyllithium in tetrahydrofuran; hexane; cyclohexane T=-90°C; 0.75 h; 2: acetaldehyde in tetrahydrofuran; hexane; cyclohexane T=-90 - 20°C; 3: With hydrogenchloride; water; ammonium chloride in tetrahydrofuran; hexane; cyclohexane T=20°C; pH=2 - 3; 1.5 h;
参考文献
Shinkaruk, Svitlana; Bennetau, Bernard; Babin, Pierre; Schmitter, Jean-Marie; Lamothe, Valerie; Bennetau-Pelissero, Catherine; Urdaci, Maria C.
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 20 p. 9383 - 9391
88440-83-9
→
反应条件
66122-70-1
反应条件
hydrogenchloride in water 20 h; Heating;
参考文献
Sibi; Miah; Snieckus
Journal of Organic Chemistry, 1984 , vol. 49, # 5 p. 737 - 742
90843-22-4
→
反应条件
66122-70-1
反应条件
aluminium trichloride in dichloromethane
参考文献
Mali; Jagtap; Patil; Pawar
Journal of the Chemical Society - Series Chemical Communications, 1992 , # 12 p. 883 - 884
63830-81-9
→
反应条件
29539-21-7
3-甲基异色烯-1-酮
+
66122-70-1
反应条件
[Me5Cp]Ir[-NHCPh2CH2O-] in tert-butyl alcohol Tishchenko reaction; 16 h; Heating;
参考文献
Suzuki, Takeyuki; Yamada, Taichiro; Watanabe, Kazuhiro; Katoh, Tadashi
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 10 p. 2583 - 2585
698-87-3
1-苯基-2-丙醇
+
201230-82-2
→
反应条件
66122-70-1
反应条件
magnesium oxide; trifluoroacetic acid; lithium chloride; palladium dichloride; Tl(OCOCF3)3 1.) 25 deg C, 1 day, 2.) MeOH, room temperature, overnight; Yield given. Multistep reaction;
参考文献
Larock, Richard C.; Fellows, Constance A.
Journal of the American Chemical Society, 1982 , vol. 104, # 7 p. 1900 - 1907
3158-74-5
2-环丙基苯甲酸
→
反应条件
17475-41-1
+
66122-70-1
反应条件
sulfuric acid T=20 - 22°C; Isomerization; 1461 h;
参考文献
Mochalov; Fedotov; Kutateladze; Trofimova; Shabarov; Zefirov
Chemistry of Heterocyclic Compounds, 1998 , vol. 34, # 3 p. 288 - 293
698-87-3
1-苯基-2-丙醇
→
反应条件
66122-70-1
反应条件
1: 50 percent / hydrogen chloride; hydrochloric acid / dioxane / 2 h / Heating 2: 82 percent / chromium trioxide / acetic acid; H2O / 2 h / 20 °C View Scheme
参考文献
Choukchou-Braham; Mostefa-Kara; Cheikh; Didi; Villemin
Synthetic Communications, 2005 , vol. 35, # 2 p. 169 - 178
147394-30-7
→
反应条件
66122-70-1
反应条件
in chloroform 6 h; Irradiation;
参考文献
Kobayashi, Kazuhiro; Konishi, Atsushi; Kanno, Yoshikazu; Suginome, Hiroshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 1 p. 111 - 116
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