三氟甲磺酸4-氰基苯基醚合成路线 (共 71 条)
反应条件
potassium phosphate; N-[(4-diphenylphosphinophenyl)methyl] D-gluconamide; PdCl2(GLCAphos)2 in water T=80°C; 16 h;
参考文献
Nishimura, Masato; Ueda, Masato; Miyaura, Norio
Tetrahedron, 2002 , vol. 58, # 29 p. 5779 - 5787
反应条件
tetrabutylammomium bromide; caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl acetamide T=90°C; 1 h;
参考文献
Rao, Maddali L.N.; Jadhav, Deepak N.; Banerjee, Debasis
Tetrahedron, 2008 , vol. 64, # 24 p. 5762 - 5772
反应条件
palladium diacetate in ethanol T=95°C; 0.25 h; microwave irradiation;
参考文献
Kabalka, George W.; Zhou, Li-Li; Naravane, Abhijit
Tetrahedron Letters, 2006 , vol. 47, # 38 p. 6887 - 6889
反应条件
palladium diacetate; 1,3-bis-(diphenylphosphino)propane; acetic acid; triethylamine 1.) DMF, 80 deg C, 16 h, 2.) DMF, 80 deg C, 6 h; Yield given. Multistep reaction;
参考文献
Larhed, Mats; Hallberg, Anders
Journal of Organic Chemistry, 1997 , vol. 62, # 22 p. 7858 - 7862
反应条件
palladium diacetate; (R)-p-tol-BINAP; sodium t-butanolate in toluene T=80°C; 12 h;
参考文献
Zheng, Nan; Christopher McWilliams; Fleitz, Fred J.; Armstrong III, Joseph D.; Volante
Journal of Organic Chemistry, 1998 , vol. 63, # 26 p. 9606 - 9607
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=90°C;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 23 p. 1729 - 1730
反应条件
tetra-n-butylammonium tetrafluoroborate; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=90°C; electrochemical reaction;
参考文献
European Journal of Organic Chemistry, , # 9 p. 1811 - 1821
反应条件
T=100°C; Substitution; 3 h;
参考文献
Synlett, , # 10 p. 1559 - 1562
反应条件
1: With Zn[N(SiMe3)2]2; tri-tert-butyl phosphine; tetrabutylammomium bromide; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=50°C; 9 h; 2: With hydrogenchloride in tetrahydrofuran; diethyl ether
参考文献
Lee, Dae-Yon; Hartwig, John F.
Organic Letters, 2005 , vol. 7, # 6 p. 1169 - 1172
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tris(dibenzylideneacetone)dipalladium (0); Ti-N complexes; sodium t-butanolate in toluene T=70°C; 1.5 h;
参考文献
Journal of the American Chemical Society, , vol. 120, # 30 p. 7651 - 7652