3,3,3-三氟-1-丙炔合成路线 (共 80 条)
反应条件
potassium hydroxide in methanol; water T=38°C; 2.5 h; Product distribution / selectivity;
参考文献
Central Glass Company, Limited
Patent: EP2143702 A1, 2010 ;
Location in patent: Page/Page column 6 ;
反应条件
bromine in acetonitrile T=50°C; 5 h;
参考文献
Journal of Fluorine Chemistry, , vol. 135, p. 114 - 128
反应条件
potassium hydroxide T=70°C; P=3750.38 Torr; 9 h; Product distribution / selectivity;
参考文献
Central Glass Company, Limited
Patent: EP2143702 A1, 2010 ;
Location in patent: Page/Page column 7 ;
反应条件
T=500°C; P=4380.18 Torr; 10 h;
参考文献
US2013/310614 A1, ;
Paragraph 0040 ;
反应条件
1: With N-chloro-succinimide; hydrogen fluoride T=0 - 20°C; Inert atmosphere; 2: With potassium fluoride T=20°C; Inert atmosphere;
参考文献
Journal of Fluorine Chemistry, , vol. 135, p. 114 - 128
反应条件
hydrogen fluoride T=-40 - 20°C; Inert atmosphere;
参考文献
Journal of Fluorine Chemistry, , vol. 135, p. 114 - 128
反应条件
N,N-dimethyl acetamide; zinc(II) chloride; zinc T=140 - 150°C;
参考文献
Canadian Journal of Chemistry, , vol. 47, p. 3093 - 3098
反应条件
1: With N-bromosuccinmide; hydrogen fluoride T=-15 - 20°C; Inert atmosphere; 2: With potassium fluoride T=20°C; Inert atmosphere;
参考文献
Journal of Fluorine Chemistry, , vol. 135, p. 114 - 128
反应条件
sulfur(IV) fluoride T=120°C;
参考文献
Journal of the American Chemical Society, , vol. 82, p. 543 - 551
Journal of the American Chemical Society, , vol. 81, p. 3165
Journal of the American Chemical Society, , vol. 82, p. 551,563
反应条件
hydrogen fluoride; 5percentTi/C T=300°C; Gas phase; Product distribution / selectivity;
参考文献
EP2028172 A1, ;
Page/Page column 6 ;