1,3,3-三甲氧基丁烷合成路线 （共 38 条）
反应条件
1-methylguanidine hydrochloride; acetyl chloride 4 h; Ambient temperature;
参考文献
Gros, Philippe; Perchec, Pierre Le; Senet, Jean-Pierre
Journal of Chemical Research, Synopses, 1995 , # 5 p. 196 - 197
参考文献
Killian; Hennion; Nieuwland
Journal of the American Chemical Society, 1934 , vol. 56, p. 1787
反应条件
diarsenic pentoxide; sulfuric acid
参考文献
Case
Journal of the American Chemical Society, 1948 , vol. 70, p. 3994
反应条件
ethanol; iron(III) chloride; zinc(II) chloride
参考文献
Bahner et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 682
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Campbell; Schaffner
Journal of the American Chemical Society, 1945 , vol. 67, p. 86,88
反应条件
potassium hydrogensulfate
参考文献
SHANGHAI FOCHON PHARMACEUTICAL CO LTD; WANG, Weibo; ZHAO, Xingdong; LEI, Ming; ZHANG, Huajie; WANG, Longcheng; ZHANG, Jian; FANG, Bo; LIU, Xia; ZHOU, Zuwen
Patent: WO2012/88680 A1, 2012 ;
Location in patent: Page/Page column 43 ;
WO 2012/088680 A1
反应条件
potassium hydroxide T=140 - 150°C;
参考文献
Nasarow; Wercholetowa; Bergelsson
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1948 , p. 511
Chem.Abstr., 1949 , p. 2577
反应条件
1: methyl vinyl ketone; trimethyl orthoformate With hydrogenchloride in 1,4-dioxane; methanol T=20°C; 168.5 h; Reflux; 2: 1,3,3-trimethoxybutane With potassium hydrogensulfate T=140°C;
参考文献
SHANGHAI FOCHON PHARMACEUTICAL CO LTD; WANG, Weibo; ZHAO, Xingdong; ZOU, Chunlan; ZHANG, Huajie; ZHANG, Weipeng; LIU, Caiping; TIAN, Qiang
Patent: WO2012/88677 A1, 2012 ;
Location in patent: Page/Page column 44 ;
参考文献
du Pont de Nemours and Co.
Patent: US2189529 , 1935 ;
参考文献
du Pont de Nemours and Co.
Patent: US2189529 , 1935 ;
反应条件
diarsenic pentoxide; sulfuric acid; water
参考文献
Campbell et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1556,1558
Journal of the American Chemical Society, 1947 , vol. 69, p. 1465
