((E)-1,2-二溴乙烯基)-苯合成路线 （共 46 条）
反应条件
1: zinc dust; alcohol 2: absolute ether solution; sulfuryl chloride 3: sodium ethylate 4: alcoholic alkali View Scheme
参考文献
Nef
Justus Liebigs Annalen der Chemie, 1899 , vol. 308, p. 325
反应条件
copper(l) iodide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene T=110°C; 40 h;
参考文献
Schuh, Kerstin; Glorius, Frank
Synthesis, 2007 , # 15 p. 2297 - 2306
反应条件
copper(l) iodide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene T=110°C; 13 h;
参考文献
Synthesis, , # 15 p. 2297 - 2306
反应条件
potassium hydroxide; hydrogen in water
参考文献
Journal of the American Chemical Society, , vol. 104, # 6 p. 1560 - 1568
反应条件
1: zinc dust; alcohol 2: absolute diethyl ether; sodium 3: absolute diethyl ether View Scheme
参考文献
Nef
Justus Liebigs Annalen der Chemie, 1899 , vol. 308, p. 325
反应条件
potassium hydroxide; hydrogen in water
参考文献
Journal of the American Chemical Society, , vol. 104, # 6 p. 1560 - 1568
参考文献
Gillespie,D.G.; Walker,B.J.
Tetrahedron Letters, 1975 , p. 4709 - 4710
反应条件
in tetrahydrofuran T=0°C; 0.166667 h;
参考文献
Azzena, Ugo; Pittalis, Mario; Dettori, Giovanna; Pisano, Luisa; Azara, Emanuela
Journal of Organometallic Chemistry, 2007 , vol. 692, # 18 p. 3892 - 3900
反应条件
in tetrahydrofuran 1 h; Heatingreagent for metal-halogen exchange (reactions with other aliphatic dihalides); Product distribution;
参考文献
Gillespie, Donal G.; Walker, Brian J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1689 - 1695
反应条件
dihydrogen peroxide 13 h; multistep reaction; various amounts of Ph2PLi (2 equiv and 1 equiv), reaction with lithium diphenylarsenide; Product distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 8 p. 1689 - 1695
