2-吡啶基(2-噻吩基)甲酮合成路线 （共 5 条）
反应条件
tert.-butylhydroperoxide; tetrabutyl-ammonium chloride; sodium carbonate; copper dichloride; BQC in water
T=40°C; 24 h;
参考文献
Boudreau, Josee; Doucette, Mike; Ajjou, Abdelaziz Nait
Tetrahedron Letters, 2006 , vol. 47, # 11 p. 1695 - 1698
反应条件
in tetrahydrofuran
T=-78°C; 1 h;
参考文献
Katritzky, Alan R.; Le, Khanh N. B.; Khelashvili, Levan; Mohapatra, Prabhu P.
Journal of Organic Chemistry, 2006 , vol. 71, # 26 p. 9861 - 9864
反应条件
1: With n-butyllithium in diethyl ether; hexane
T=-78 - 0°C; 0.5 h;
2: With hydrogenchloride in diethyl ether; hexane
pH=1; 0.5 h;
参考文献
Jakobsen, Palle; Madsen, Peter; Andersen, HenrikSune
European Journal of Medicinal Chemistry, 2003 , vol. 38, # 4 p. 357 - 362
反应条件
in tetrahydrofuran
1 h; Inert atmosphere;
参考文献
Rao, G. Venkateswara; Swamy, B. Narayana; Kumar, P. Hareesh; Reddy, G. Chandrasekara
Synthetic Communications, 2009 , vol. 39, # 10 p. 1835 - 1846
参考文献
Olea-Azar; Abarca; Norambuena; Opazo; Rigol; Ballesteros; Chadlaoui
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2005 , vol. 61, # 9 p. 2261 - 2266
