二苯基碘三氟甲烷磺酸盐合成路线 （共 201 条）
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=0 - 20°C; 0.5 h;
参考文献
Jalalian, Nazli; Petersen, Tue B.; Olofsson, Berit
Chemistry--A European Journal, 2012 , vol. 18, # 44 p. 14140 - 14149,10
反应条件
dihydrogen peroxide; cyclohexene in methanol oxidative anion metathesis; Heating;
参考文献
Phipps, Robert J.; Grimster, Neil P.; Gaunt, Matthew J.
Journal of the American Chemical Society, 2008 , vol. 130, # 26 p. 8172 - 8174
反应条件
iodine; 3-chloro-benzenecarboperoxoic acid in dichloromethane T=80°C; 0.166667 h; Product distribution; Further Variations:Temperaturesreaction times;
参考文献
Jalalian, Nazli; Petersen, Tue B.; Olofsson, Berit
Chemistry--A European Journal, 2012 , vol. 18, # 44 p. 14140 - 14149,10
反应条件
1: bromobenzene With n-butyllithium in diethyl ether; hexane; toluene T=-78°C; Metallation; 0.25 h; 2: Trifluoro-methanesulfonatephenyl-((E)-2-trifluoromethanesulfonyloxy-vinyl)-iodonium; in diethyl ether; hexane; toluene T=-78 - 20°C; Substitution; Decomposition;
参考文献
Pirguliyev, Namig Sh; Brel, Valery K.; Akhmedov, Navruz G.; Zefirov, Nikolai S.
Synthesis, 2000 , # 1 p. 81 - 83
反应条件
1: iodobenzene; benzene With dipotassium peroxodisulfate; trifluoroacetic acid in dichloromethane T=36 - 38°C; 20 h; 2: sodium trifluoro-methanesulfonate in water T=20°C; 8 h;
参考文献
Hossain, Md. Delwar; Kitamura, Tsugio
Tetrahedron, 2006 , vol. 62, # 29 p. 6955 - 6960
反应条件
1: trifluorormethanesulfonic acid; [bis(acetoxy)iodo]benzene in dichloromethane T=0 - 20°C; Inert atmosphereDarkness; 2: benzene in dichloromethane T=0 - 20°C; Inert atmosphereDarkness;
参考文献
Wang, Bijia; Cerny, Ronald L.; Uppaluri, Shriharsha; Kempinger, Jayson J.; Dimagno, Stephen G.
Journal of Fluorine Chemistry, 2010 , vol. 131, # 11 p. 1113 - 1121
反应条件
1: trifluoromethylsulfonic anhydride With urea hydrogen peroxide addition compound in dichloromethane; 2,2,2-trifluoroethanol T=0°C; 0.5 h; 2: iodobenzene in dichloromethane; 2,2,2-trifluoroethanol T=0°C; 3: benzene in dichloromethane; 2,2,2-trifluoroethanol T=0 - 40°C;
参考文献
Merritt, Eleanor A.; Malmgren, Joel; Klinke, Felix J.; Olofsson, Berit
Synlett, 2009 , # 14 p. 2277 - 2280
反应条件
in acetonitrile T=20°C; Substitution; 2 h;
参考文献
Watanabe, Shin-Ichi; Yamamoto, Keiichirou; Itagaki, Yukiko; Iwamura, Tatsunori; Iwama, Tetsuo; Kataoka, Tadashi
Tetrahedron, 2000 , vol. 56, # 6 p. 855 - 863
反应条件
in benzene T=-30 - 20°C; 5 h;
参考文献
Krief, Alain; Dumont, Willy; Robert, Michael
Synlett, 2006 , # 3 p. 484 - 486
反应条件
in dichloromethane T=20°C; Substitution;
参考文献
Carroll, Michael A.; Pike, Victor W.; Widdowson, David A.
Tetrahedron Letters, 2000 , vol. 41, # 28 p. 5393 - 5396
