hydrogen; palladium dihydroxide in tetrahydrofuran; methanol P=3102.9 Torr; 10.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 116, # 18 p. 8126 - 8132
1: With ruthenium trichloride; sodium periodate in tetrachloromethane; water; acetonitrile 2 h; 2: With hydrogenchloride in tetrahydrofuran 12 h; Heating;
参考文献
Badorrey, Ramon; Cativiela, Carlos; Diaz-de-Villegas, Maria D.; Diez, Roberto; Galvez, Jose A.
European Journal of Organic Chemistry, 2002 , # 22 p. 3763 - 3767
pyridoxal 5'-phosphate in water; tert-butyl alcohol T=40°C; 4 h; alcalase, pH=8.5; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 59, # 25 p. 7580 - 7581
1: With lithium carbonate in water; tert-butyl alcohol T=23°C; 0.166667 h; Resolution of racemate; 2: With 2-hydroxymethyl-pyridine; Alcalase; water; Zn(CH3COO)2*2H2O in tert-butyl alcohol T=23°C; 4 h; Resolution of racemateEnzymatic reaction; optical yield given as percent ee;
