in acetone
to acetone soln. of Rh complex the ligand added with stirring, if necessary refluxed for 2 h; crystals washed with acetone, dried in vac.; elem. anal.;
参考文献
Halesha, R.; Reddy, G.K.N.; Rao, S.P. Sudhakar; Manohar, H.
Journal of Organometallic Chemistry, 1983 , vol. 252, # 2 p. 231 - 242
in acetone
to acetone soln. of Rh complex the ligand added with stirring, if necessary refluxed for 2 h; crystals washed with acetone, dried in vac.; elem. anal.;
参考文献
Halesha, R.; Reddy, G.K.N.; Rao, S.P. Sudhakar; Manohar, H.
Journal of Organometallic Chemistry, 1983 , vol. 252, # 2 p. 231 - 242
in acetone
to acetone soln. of Rh complex the ligand added with stirring, if necessary refluxed for 2 h; crystals washed with acetone, dried in vac.; elem. anal.;
参考文献
Halesha, R.; Reddy, G.K.N.; Rao, S.P. Sudhakar; Manohar, H.
Journal of Organometallic Chemistry, 1983 , vol. 252, # 2 p. 231 - 242
in methanol
dropwise addn. of soln. of VOSO4 to soln of bromanilic acid, addn. of soln. of N-ligand (stirring, room temp.), refluxing (8 h; crystn.); filtration, washing (MeOH, Et2O), drying (vac., over P2O5), recrystn. (DMF/EtOH); elem. anal.;
参考文献
Li, Yan-Tuan; Yan, Cui-Wei; Xu, Cheng-Shui
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1999 , vol. 29, # 6 p. 995 - 1007
