反应条件
1.1: zinc; TMSCl; 1,2-dibromoethane / dimethylformamide / 0.33 h / 60 °C 1.2: 100 percent / CuCN; LiCl / dimethylformamide / -55 - 0 °C 2.1: BH3*SMe2 / tetrahydrofuran / 0 - 20 °C 2.2: 68.3 percent / H2O2; NaOAc / H2O; tetrahydrofuran / 12 h / 20 °C View Scheme
参考文献
Shimasaki, Yasuharu; Kiyota, Hiromasa; Sato, Minoru; Kuwahara, Shigefumi
Synthesis, 2005 , # 19 art. no. C07305SS, p. 3191 - 3192
