N-(2-甲酰基苯基)-4-甲基苯磺酰胺合成路线 （共 24 条）
反应条件
1.1: iodine; caesium carbonate / acetonitrile / 9 h / 23 - 25 °C
1.2: 6 h / 23 - 25 °C
2.1: AlCl3, aluminium chloride / benzene / 9 h / Reflux
3.1: acetonitrile / 12 h / Inert atmosphere; Reflux
View Scheme
参考文献
Ali, Shaukat; Li, Ying-Xiu; Anwar, Saeed; Yang, Fang; Chen, Zi-Sheng; Liang, Yong-Min
Journal of Organic Chemistry, 2012 , vol. 77, # 1 p. 424 - 431
反应条件
1.1: iodine; caesium carbonate / acetonitrile / 9 h / 23 - 25 °C
1.2: 6 h / 23 - 25 °C
2.1: AlCl3, aluminium chloride / benzene / 9 h / Reflux
View Scheme
参考文献
Ali, Shaukat; Li, Ying-Xiu; Anwar, Saeed; Yang, Fang; Chen, Zi-Sheng; Liang, Yong-Min
Journal of Organic Chemistry, 2012 , vol. 77, # 1 p. 424 - 431
反应条件
1: L-proline / methanol / 24 h / |Reflux
2: iodine; potassium carbonate / methanol / 4 h / 0 °C
3: sodium hydroxide / methanol; water / |Reflux
View Scheme
参考文献
Gao, Wen-Chao; Jiang, Shan; Wang, Ruo-Lin; Zhang, Chi
Chemical Communications, 2013 , vol. 49, # 43 p. 4890 - 4892
反应条件
1.1: (S)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine / chloroform / 30 h / 20 °C
2.1: silica gel / chloroform / 24 h / 20 °C
2.2: 3 h / 20 °C
View Scheme
参考文献
Zhang, Xinshuai; Song, Xixi; Li, Hao; Zhang, Shilei; Chen, Xiaobei; Yu, Xinhong; Wang, Wei
Angewandte Chemie - International Edition, 2012 , vol. 51, # 29 p. 7282 - 7286
