2-环己基氨基-1-苯基乙醇合成路线 (共 11 条)
反应条件
Sulfated tungstate T=70°C; 0.5 h; Green chemistry; regioselective reaction;
参考文献
Pathare, Sagar P.; Akamanchi, Krishnacharya G.
Tetrahedron Letters, 2013 , vol. 54, # 48 p. 6455 - 6459
反应条件
in water T=20°C; 14 h;
参考文献
Organic Letters, , vol. 7, # 17 p. 3649 - 3651
反应条件
sodium hydroxide in diethylene glycol T=130 - 140°C;
参考文献
Wrobel; Bobin; Karczewski
Polish Journal of Chemistry, 2006 , vol. 80, # 6 p. 907 - 912
反应条件
sodium tetrahydroborate in methanol 0.5 h; Ambient temperature;
参考文献
Alcaide, Benito; Escobar, Gerardo; Perez-Ossorio, Rafael; Plumet, Joaquin; Sanz, Dionisia
Journal of Chemical Research, Miniprint, 1984 , # 5 p. 1466 - 1488
反应条件
1: benzene / 0.17 h / Ambient temperature 2: 68 percent / NaBH4 / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 5 p. 1466 - 1488
反应条件
1: 54 percent / tert-BuOK / dimethylformamide / 48 h / 20 °C 2: 95 percent / NaOH / bis-(2-hydroxy-ethyl) ether / 130 - 140 °C View Scheme
参考文献
Polish Journal of Chemistry, , vol. 80, # 6 p. 907 - 912
反应条件
1: benzene / 0.17 h / Ambient temperature 2: 68 percent / NaBH4 / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 5 p. 1466 - 1488
反应条件
1: benzene / 0.25 h / Ambient temperature 2: 68 percent / NaBH4 / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 5 p. 1466 - 1488
反应条件
triphenylphosphine; diethylazodicarboxylate in diethyl ether 18 h; Ambient temperature;
参考文献
Pfister, Juerg R.
Synthesis, 1984 , # 11 p. 969 - 970
反应条件
in toluene
18 h; Heating;
参考文献
Irwin; Wheeler; Harper
Journal of medicinal chemistry, 1972 , vol. 15, # 4 p. 445 - 446