反应条件
1: 1.) tri-n-butyltin hydride, azobis(isobutyronitrile), 2.) NaOH / 1.) 130 deg C, 76 h, 2.) H2O, heating, 2 h
2: 93 percent / diethyl ether / 0.5 h / -20 °C
3: 62 percent / Clorox/NaOCl, RuO2*2H2O / CCl4 / 47 h
View Scheme
参考文献
Applequist, Douglas E.; Renken, Terry L.; Wheeler, James W.
Journal of Organic Chemistry, 1982 , vol. 47, # 25 p. 4985 - 4995
