(9ci)-六氢-2-氧代-1H-氮杂卓-1-羧醛合成路线 （共 11 条）
反应条件
sodium hydrogencarbonate; sodium carbonate in acetone
参考文献
Alcaide, Benito; Almendros, Pedro; Alonso, Jose M.
Chemistry - A European Journal, 2006 , vol. 12, # 10 p. 2874 - 2879
参考文献
Villa, Mathew V. J.; Targett, Sarah M.; Barnes, John C.; Whittingham, William G.; Marquez, Rodolfo
Organic Letters, 2007 , vol. 9, # 9 p. 1631 - 1633
反应条件
1: sodium formate With acetyl chloride in diethyl ether
T=20°C; Inert atmosphere;
2: epsilon-caprolactam in diethyl ether
T=60°C; Inert atmosphere;
参考文献
Mathieson, Jennifer E.; Crawford, James J.; Schmidtmann, Marc; Marquez, Rodolfo
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 10 p. 2170 - 2175
反应条件
in acetonitrile
Irradiation;
参考文献
Quazzani-Chadi, Laila; Quirion, Jean-Charles; Troin, Yves; Gramain, Jean-Claude
Tetrahedron, 1990 , vol. 46, # 23 p. 7751 - 7762
反应条件
ruthenium trichloride; sodium periodate in 1,2-dichloro-ethane
T=20°C;
参考文献
Alcaide, Benito; Almendros, Pedro; Alonso, Jose M.
Chemistry - A European Journal, 2006 , vol. 12, # 10 p. 2874 - 2879
反应条件
1: 72 percent / [(PCy3)2Cl2Ru=CHPh] / toluene / 110 °C
2: NaIO4; aq. RuCl3 / 1,2-dichloro-ethane / 20 °C
View Scheme
参考文献
Alcaide, Benito; Almendros, Pedro; Alonso, Jose M.
Chemistry - A European Journal, 2006 , vol. 12, # 10 p. 2874 - 2879
参考文献
Gramain, J. C.; Remuson, R.
Synthesis, 1982 , # 4 p. 264 - 266
反应条件
triethylamine tris(hydrogen fluoride) in acetonitrile
5 h; electrolysis;
参考文献
Sono, Masakazu; Toyoda, Naoko; Shimizu, Kahori; Noda, Eiji; Shizuri, Yoshikazu; Tori, Motoo
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 6 p. 1141 - 1145
反应条件
sodium periodate; RuO4 in tetrachloromethane; water
72 h; Ambient temperature;
参考文献
Tangari, Nicola; Giovine, Maria; Morlacchi, Flaviano; Vetuschi, Claudio
Gazzetta Chimica Italiana, 1985 , vol. 115, # 6 p. 325 - 328
反应条件
ruthenium(IV) oxide; sodium periodate in ethyl acetate
71 h; Ambient temperature;
参考文献
Yoshifuji, Shigeyuki; Arakawa, Yukimi; Nitta, Yoshihiro
Chemical & Pharmaceutical Bulletin, 1987 , vol. 35, # 1 p. 357 - 363
