4-硝基-2,1,3-苯并噻二唑合成路线 （共 16 条）
反应条件
sulfuric acid; nitric acid Nitration;
参考文献
Murashima, Takashi; Shiga, Daiki; Nishi, Keiji; Uno, Hidemitsu; Ono, Noboru
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 16 p. 2671 - 2675
反应条件
trithiazyl trichloride in tetrachloromethane; benzene Ambient temperature;
参考文献
Domschke, Guenter; Heimbold, Ilka
Zeitschrift fuer Chemie (Stuttgart, Germany), 1987 , vol. 27, # 1 p. 31 - 32
反应条件
trithiazyl trichloride in benzene Ambient temperature;
参考文献
Domschke, Guenter; Heimbold, Ilka
Zeitschrift fuer Chemie (Stuttgart, Germany), 1987 , vol. 27, # 1 p. 31 - 32
参考文献
Zhurnal Obshchei Khimii, , vol. 23, p. 1552,1554; engl. Ausg. S. 1629
Zhurnal Obshchei Khimii, , vol. 20, p. 1914,1916; engl. Ausg. S. 1981, 1983
反应条件
1: SOCl2; toluene 2: HNO3; concentrated H2SO4 View Scheme
参考文献
Zhurnal Obshchei Khimii, , vol. 23, p. 1552,1554; engl. Ausg. S. 1629
Zhurnal Obshchei Khimii, , vol. 20, p. 1914,1916; engl. Ausg. S. 1981, 1983
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 53, p. 530 - 537
Zhurnal Obshchei Khimii, , vol. 53, p. 612 - 619
反应条件
hydrogen in tetrahydrofuran; water T=120°C; P=37503.8 Torr; 18 h; chemoselective reaction;
参考文献
Jagadeesh, Rajenahally V.; Surkus, Annette-Enrica; Junge, Henrik; Pohl, Marga-Martina; Radnik, Joerg; Rabeah, Jabor; Huan, Heming; Schunemann, Volker; Brueckner, Angelika; Beller, Matthias
Science, 2013 , vol. 342, # 6162 p. 1073 - 1076
反应条件
chlorine; iron T=120°C;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 2, p. 405 - 407
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 2, # 4 p. 541 - 544
反应条件
1: 92 percent / hydroxylamine hydrochloride; potassium hydroxide / methanol / -15 - 20 °C 2: potassium hydroxide; aq. sodium hypochlorite / ethanol / 1 h / -10 - 20 °C 3: 67 percent / triethyl phosphite / 1 h / Heating View Scheme
参考文献
Cillo, Catherine M.; Lash, Timothy D.
Journal of Heterocyclic Chemistry, 2004 , vol. 41, # 6 p. 955 - 962
反应条件
potassium hydroxide; hydroxylamine hydrochloride in methanol T=-15 - 20°C;
参考文献
Cillo, Catherine M.; Lash, Timothy D.
Journal of Heterocyclic Chemistry, 2004 , vol. 41, # 6 p. 955 - 962
