1-(4-硝基苯基)哌啶合成路线 (共 39 条)
反应条件
in pyridine T=80°C; 5 h;
参考文献
Matsumura, Eizo; Tohda, Yasuo; Ariga, Masahiro
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 7 p. 2174 - 2180
反应条件
cerium (IV) sulfate; sodium nitrite in water T=20°C; 1 h;
参考文献
Synthetic Communications, , vol. 37, # 19 p. 3381 - 3392
反应条件
dimethylsulfide borane complex in tetrahydrofuran 9 h; Heating;
参考文献
Venuti, Michael C.; Ort, Oswald
Synthesis, 1988 , # 12 p. 985 - 988
反应条件
(ethylenedinitrilo)tetraacetic acid disodium salt; mercury(II) oxide in water; dimethyl sulfoxide T=100°C; 1 h;
参考文献
Archiv der Pharmazie, , vol. 315, # 2 p. 119 - 131
反应条件
in methanol; water 19 h; Ambient temperatureIrradiation;
参考文献
Cervello, J.; Figueredo, M.; Marquet, J.; Moreno-Manas, M.; Bertran, J.; Lluch, J. M.
Tetrahedron Letters, 1984 , vol. 25, # 37 p. 4147 - 4150
参考文献
Morton-Norwich Products, Inc.
Patent: US3947434 A1, 1976 ;
反应条件
1: Et3N / CH2Cl2 2: 98 percent / 1 h / 20 °C View Scheme
参考文献
Synlett, , # 10 p. 1559 - 1562
反应条件
1: 85 percent / N,N-dimethylaniline / diethyl ether; tetrahydrofuran / 1 h / Heating 2: 46 percent / 10M Me2S*BH3 / tetrahydrofuran / 9 h / Heating View Scheme
参考文献
Synthesis, , # 12 p. 985 - 988
反应条件
1: 85 percent / N,N-dimethylaniline / diethyl ether; tetrahydrofuran / 1 h / Heating 2: 46 percent / 10M Me2S*BH3 / tetrahydrofuran / 9 h / Heating View Scheme
参考文献
Synthesis, , # 12 p. 985 - 988
反应条件
1: 29.3 percent / NaBH4 / methanol / 1.) room temp., 16 h, reflux 1 h 2: 8 percent / HgO, Na2EDTA / dimethylsulfoxide; H2O / 1 h / 100 °C View Scheme
参考文献
Archiv der Pharmazie, , vol. 315, # 2 p. 119 - 131