potassium hydroxide; tetra-n-octylammonium bromide in water; benzene T=20 - 22°C; 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Russian Journal of Organic Chemistry, , vol. 33, # 4 p. 467 - 474
potassium hydroxide in toluene T=18 - 22°C; 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 40, # 4.1 p. 739 - 743
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 4 p. 842 - 846
1: 45 percent / conc. H2SO4 / 33 h / 50 °C 3: pyridinium chlorochromate / CH2Cl2 / 2.5 h / 14 - 16 °C 4: KOH / toluene / 3 h / 18 - 22 °C View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 40, # 4.1 p. 739 - 743
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 4 p. 842 - 846
2: pyridinium chlorochromate / CH2Cl2 / 2.5 h / 14 - 16 °C 3: KOH / toluene / 3 h / 18 - 22 °C View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 40, # 4.1 p. 739 - 743
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 4 p. 842 - 846
