1-溴-4,4-二甲基戊烷合成路线 (共 16 条)
反应条件
magnesium 1) ether; Yield given. Multistep reaction;
参考文献
Schulz; Sprung; Kroning
Pharmazie, 1983 , vol. 38, # 5 p. 310 - 313
反应条件
1: aqueous ethanol View Scheme
参考文献
Gutman; Hickinbottom
Journal of the Chemical Society, 1951 , p. 3344,3347
反应条件
ethanol Verseifen des Reaktionsprodukts mit alkoh.KOH;
参考文献
Mallinckrodt Chem.Works
Patent: US2032159 , 1933 ;
反应条件
1: 70 percent / Na/C2H5OH / 6 h / Heating View Scheme
参考文献
Lynch,E.R.; McCall,E.B.
Journal of the Chemical Society, 1960 , p. 1254 - 1262
反应条件
potassium permanganate Multistep reaction;
参考文献
Brumby, Steven
Journal of Physical Chemistry, 1983 , vol. 87, # 11 p. 1917 - 1924
反应条件
Ascaridole; hydrogen bromide
参考文献
Kharasch; Hannum; Gladstone
Journal of the American Chemical Society, 1934 , vol. 56, p. 244
反应条件
pyridine; phosphorus tribromide
Bromination; 12 h; Heating;
参考文献
Hamano, Hiroshi; Nagata, Keiichi; Fukada, Nobuo; Shimotahira, Hiroshi; Ju, Xiu-Lian; Ozoe, Yoshihisa
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 3 p. 665 - 674
反应条件
1: platinum oxide / Hydrogenation
2: diethyl ether; PBr3 / anfangs unter Kuehlung, dann bei 40-50grad
View Scheme
参考文献
Bartlett; Rosen
Journal of the American Chemical Society, 1942 , vol. 64, p. 544
反应条件
1: diethyl ether
2: platinum oxide / Hydrogenation
3: diethyl ether; PBr3 / anfangs unter Kuehlung, dann bei 40-50grad
View Scheme
参考文献
Bartlett; Rosen
Journal of the American Chemical Society, 1942 , vol. 64, p. 544
反应条件
1: zinc; boiling ethanol / in praktisch quantitativer Ausbeute
2: HBr
View Scheme
参考文献
Whitmore; Homeyer
Journal of the American Chemical Society, 1933 , vol. 55, p. 4558