2-(4-溴苯基)-2-氧代硫氰酸乙酯合成路线 (共 21 条)
反应条件
in ethanol; water T=20°C; 7 h;
参考文献
US2008/45556 A1, ;
Page/Page column 15 ;
US2008/45578 A1, ;
Page/Page column 15 ;
反应条件
1: ammonium thiocyanate With montmorillonite K10 clay in acetone T=20°C; 0.666667 h; 2: 2-bromo-1-(4-bromophenyl)-1-ethanone T=20°C; 0.00833333 h; Neat (no solvent)Grinding;
参考文献
Tetrahedron Letters, , vol. 53, # 14 p. 1780 - 1785
反应条件
N-bromosuccinmide in acetonitrile T=20°C; 7 h;
参考文献
Tetrahedron Letters, , vol. 52, # 13 p. 1432 - 1435
反应条件
tetrabutylammomium bromide in water T=20°C; 0.583333 h;
参考文献
Chinese Chemical Letters, , vol. 22, # 3 p. 300 - 302
反应条件
cis-1,4-bis(triphenylphosphonium)-2-butene peroxodisulfate; oxygen in methanol T=0°C; 1.08333 h;
参考文献
Synthetic Communications, , vol. 42, # 14 p. 2058 - 2066
反应条件
1: para-bromoacetophenone With PhI(ODNs)OH in acetonitrile T=80°C; 1 h; 2: [C4mim][SCN] in acetonitrile T=20°C; 0.166667 h;
参考文献
Journal of the Chinese Chemical Society, , vol. 55, # 6 p. 1204 - 1207
反应条件
in water T=20°C; 0.5 h;
参考文献
Chinese Chemical Letters, , vol. 22, # 6 p. 659 - 662
反应条件
in neat (no solvent) T=30°C; 4 h;
参考文献
RSC Advances, , vol. 4, # 27 p. 14297 - 14303
反应条件
1-methyl-1H-imidazole 2 h;
参考文献
Organic Letters, , vol. 11, # 15 p. 3382 - 3385
参考文献
Journal of the American Chemical Society, , vol. 61, p. 1830
Roczniki Chemii, , vol. 10, p. 555,561
Chem. Zentralbl., , vol. 101, # II p. 3274