2,3,4,6-四-o-苄基-D-吡喃葡萄糖合成路线 （共 109 条）
反应条件
N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium 1.) Et2O, cyclohexane, isopentane, -78 deg C, 4 h, 2.) Et2O, cyclohexane, isopentane, -78 deg C, 90 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Synthesis, , # 2 p. 176 - 182
反应条件
in tetrahydrofuran 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mangholz, Sissi E.; Vasella, Andrea
Helvetica Chimica Acta, 1991 , vol. 74, # 8 p. 2100 - 2111
反应条件
in tetrahydrofuran 5 h; Ambient temperatureIrradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Helvetica Chimica Acta, , vol. 74, # 8 p. 2100 - 2111
反应条件
diisobutylaluminium hydride in dichloromethane T=0°C; 0.0833333 h; Product distribution; Further Variations:Temperatures;
参考文献
Journal of Carbohydrate Chemistry, , vol. 23, # 4 p. 253 - 259
反应条件
diisobutylaluminium hydride in dichloromethane T=0°C; 0.0833333 h; Product distribution; Further Variations:SolventsTemperatures;
参考文献
Journal of Carbohydrate Chemistry, , vol. 23, # 4 p. 253 - 259
反应条件
silver trifluoromethanesulfonate; triethylamine; 4-nitrophenylsulfonyl chloride in dichloromethane 1.) -40-0 deg C, 40 min, 2.) 0 deg C, 3 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 53, # 6 p. 1761 - 1762
反应条件
1: 92 percent / tetrabutylammonium bromide; aq. NaOH / toluene / 20 °C 2: NIS; Drierite; TfOH / toluene / 0.5 h / 20 °C View Scheme
参考文献
Tsuboyama; Takeda; Torii; Ebiiiara; Siiimizu; Suzuki; Sato; Furuhata; Ogura
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 3 p. 636 - 638
反应条件
triethylamine 1.) CH2Cl2, reflux, 2 h, 2.) CH2Cl2, MeOH, overnight; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
McAdam, David P.; Stick, Robert V.
Australian Journal of Chemistry, 1988 , vol. 41, # 4 p. 563 - 573
反应条件
diethyl-trichloromethyl-amine 1.) dichloromethane, 25 deg C, 3 h, 2.) dichloromethane, reflux, 5 d; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Copeland, Christopher; McAdam, David P.; Stick, Robert V.
Australian Journal of Chemistry, 1983 , vol. 36, # 6 p. 1239 - 1247
反应条件
silver trifluoromethanesulfonate; triethylamine; 4-nitrophenylsulfonyl chloride in dichloromethane 1.) -40-0 deg C, 40 min, 2.) 0 deg C, 3 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 53, # 6 p. 1761 - 1762
