in deuterated toluene
Me2NBCl2 and C7H8-d8 were placed in a NMR tube; the tube was evacuated at -196°C and Me2AsNMe2 condensed into it; the tube was sealed and agitated gently at -90°C; NMR study of the reaction from -90°C to 25°C;; not isolated, detected by (11)B-, (13)C-, and (1)H-NMR spectroscopy;;
参考文献
Krannich, Larry K.; Kanjolia, Ravindra K.; Watkins, Charles L.
Journal of the Indian Chemical Society, 1985 , vol. 62, # 11 p. 795 - 799
in tetrachloromethane
under N2, with exclusion of moisture, added soln. of org. compd. to boron compd. soln. (1/2 mol ratio); sepd. by fractional distn.;
参考文献
Haubold, Wolfgang; Zurmuehl, Konrad
Chemische Berichte, 1980 , vol. 113, # 7 p. 2333 - 2341
