6-甲基水杨酸乙酯/2-羟基-6-甲基苯甲酸乙酯合成路线 （共 27 条）
反应条件
boron tribromide in dichloromethane T=-78°C; 0.5 h;
参考文献
Journal of the American Chemical Society, , vol. 127, # 24 p. 8872 - 8888
反应条件
sodium acetate in acetic acid
反应条件
bromine in tetrachloromethane; acetic acid 1.) ice bath, 30 min; 2.) reflux, 16 h;
参考文献
Synthesis, , # 10 p. 814 - 815
反应条件
dipotassium peroxodisulfate; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; trifluoroacetic acid; trifluoroacetic anhydride T=80°C; 11 h;
参考文献
Organic Letters, , vol. 14, # 11 p. 2874 - 2877
反应条件
1: With sodium ethanolate Condensation; cyclization; 2: With lithium chloride; copper dichloride in N,N-dimethyl-formamide T=90°C; Aromatisation;
参考文献
Journal of Natural Products, , vol. 62, # 12 p. 1627 - 1631
反应条件
1: With bromine in tetrachloromethane; acetic acid T=0 - 20°C; 1.5 h; 2: in tetrachloromethane; acetic acid T=98°C;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 43, # 8 p. 1729 - 1736
反应条件
copper diacetate; manganese triacetate in acetic acid 36 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 53, # 10 p. 2137 - 2143
反应条件
trimethylsilyl trifluoromethanesulfonate; [VO(OEt)Cl2] in ethanol 1) 1 h, 0 deg C 2) 1 h, r.t.; Yield given. Yields of byproduct given;
参考文献
Chemistry Letters, , # 5 p. 783 - 784
反应条件
trimethylsilyl trifluoromethanesulfonate in ethanol 1) 1 h, 0 deg C 2) 1 h, r.t.; Yield given. Yields of byproduct given;
参考文献
Chemistry Letters, , # 5 p. 783 - 784
反应条件
copper diacetate; manganese triacetate; acetic acid; zinc 1.) RT, 36 h, glacial acetic acid, 2.) 25 deg C, 5 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 53, # 10 p. 2137 - 2143
