2,4,6-三异丙基苯磺酰氯合成路线 (共 18 条)
反应条件
chlorosulfonic acid in chloroform T=0°C;
参考文献
Mase, Nobuyuki; Watanabe, Yoshihiko; Ueno, Yoshio; Toru, Takeshi
Journal of Organic Chemistry, 1997 , vol. 62, # 22 p. 7794 - 7800
反应条件
hydrazine in tetrahydrofuran T=-10 - 0°C; 3 h;
参考文献
Yang, Ming-Hsiu; Matikonda, Siddharth S.; Altman, Ryan A.
Organic Letters, 2013 , vol. 15, # 15 p. 3894 - 3897
反应条件
in dichloromethane 1 h; Ambient temperature;
参考文献
Dabkowski, W.; Michalski, J.; Skrzypczynski, Z.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 26, p. 321 - 326
反应条件
sodium azide in ethanol 19 h; Ambient temperature;
参考文献
Stone, Martin J.; Dyk, Martha S. van; Booth, Paul M.; Williams, Dudley H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 7 p. 1629 - 1635
反应条件
in dichloromethane 1 h; Ambient temperature;
参考文献
Dabkowski, W.; Michalski, J.; Skrzypczynski, Z.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 26, p. 321 - 326
反应条件
dichloro bis(acetonitrile) palladium(II); copper acetylacetonate; copper (I) cyanide; sodium carbonate in 1,4-dioxane T=130°C; 24 h; Sealed tubeAir;
参考文献
Chen, Jianbin; Sun, Yang; Liu, Bin; Liu, Dongfang; Cheng, Jiang
Chemical Communications, 2012 , vol. 48, # 3 p. 449 - 451
反应条件
hydrogenchloride; zinc
参考文献
Garratt, Dennis G.; Beaulieu, Pierre L.
Canadian Journal of Chemistry, 1980 , vol. 58, # 24 p. 2738 - 2744
反应条件
triethylamine in dichloromethane T=25°C; 24 h;
参考文献
Suwinski, Jerzy; Salwinska, Ewa
Tetrahedron, 1994 , vol. 50, # 19 p. 5741 - 5752
反应条件
ammonium hydroxide in chloroform T=20°C; 2 h;
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 45 p. 6125 - 6128
反应条件
sodium hydride in tetrahydrofuran T=0°C; 16 h;
参考文献
Nishimoto, Atsushi; Jitsuzaki, Daichi; Onizuka, Kazumitsu; Taniguchi, Yosuke; Nagatsugi, Fumi; Sasaki, Shigeki
Nucleic Acids Research, 2013 , vol. 41, # 13 p. 6774 - 6781