Burton, Graham W.; Daroszewski, Janusz; Nickerson, James G.; Johnston, James B.; Mogg, Trevor J.; Nikiforov, Grigory B.
Canadian Journal of Chemistry, 2014 , vol. 92, # 4 p. 305 - 316
potassium hydroxide in methanol; water
0.5 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
lithium aluminium tetrahydride in diethyl ether
1 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C
2: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 °C / |Inert atmosphere
View Scheme
参考文献
Burton, Graham W.; Daroszewski, Janusz; Nickerson, James G.; Johnston, James B.; Mogg, Trevor J.; Nikiforov, Grigory B.
Canadian Journal of Chemistry, 2014 , vol. 92, # 4 p. 305 - 316