1-(4-氯苯基)-3-(4-甲氧基苯基)-2-丙烯-1-酮合成路线 (共 11 条)
反应条件
zinc oxide T=25 - 30°C; Friedel-Crafts Acylation; 2.16667 h; regioselective reaction;
参考文献
More, Parmeshwar E.; Bandgar, Babasaheb P.; Kamble, Vinod T.
Catalysis Communications, 2012 , vol. 27, p. 30 - 32
反应条件
sodium hydroxide in ethanol 3 h;
参考文献
Hazarkhani, Hassan; Kumar, Pradeep; Kondiram, Kadam Sachin; Shafi Gadwal, Ikhlas M.
Synthetic Communications, 2010 , vol. 40, # 19 p. 2887 - 2896
反应条件
triethylamine; 4-amino-5-phenyl-4H-1,2,4-triazole-3-thiol in ethanol 5 h; Heating;
参考文献
Holla, B Shivarama; K, Shridhara; Kalluraya, Balakrishna
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 7 p. 672 - 675
反应条件
1: sodium periodate; osmium(VIII) oxide; N-benzyl-N,N,N-triethylammonium chloride / tetrahydrofuran; water / 100 °C / Microwave irradiation 2: sodium hydroxide / methanol; water / 55 °C / Microwave irradiation View Scheme
参考文献
Medicinal Chemistry Research, , vol. 21, # 6 p. 922 - 931
反应条件
4-tolylthallium(III) bis(trifluoroacetate); titanium tetrachloride 1.) benzene, RT, 30 min, 2.) THF, -78 deg C, 1.5 h, RT, 1 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 53, # 5 p. 1022 - 1025
反应条件
in tetrahydrofuran T=55°C; 3 h; Product distributionMechanism;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 5 p. 1741 - 1746
反应条件
1: NH2OH*HCl; TEA 2: MnO2 / CHCl3 / Heating View Scheme
参考文献
Kurangi, Reshma F.; Kawthankar, Rima; Sawal, Sulfala; Desai, Vidya G.; Tilve, Santosh G.
Synthetic Communications, 2007 , vol. 37, # 4 p. 587 - 589
反应条件
p-MeOC6H4-IDMg in tetrahydrofuran T=55°C; 3 h; Further byproducts given;
参考文献
Okubo, Masao; Yoshida, Shunsei; Egami, Yoshiji; Matsuo, Koji; Nagase, Shigeru
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 5 p. 1741 - 1746
反应条件
in tetrahydrofuran T=55°C; 3 h; Further byproducts given;
参考文献
Okubo, Masao; Yoshida, Shunsei; Egami, Yoshiji; Matsuo, Koji; Nagase, Shigeru
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 5 p. 1741 - 1746
反应条件
in tetrahydrofuran T=55°C; 3 h; Product distributionMechanism;
参考文献
Okubo, Masao; Yoshida, Shunsei; Egami, Yoshiji; Matsuo, Koji; Nagase, Shigeru
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 5 p. 1741 - 1746