1-(4-甲基苯基)-1-甲基乙胺合成路线 （共 7 条）
参考文献
Sankyo Company, Limited
Patent: US5536714 A1, 1996 ;
反应条件
cerium(III) chloride in tetrahydrofuran T=-50°C; 1.) 1 h, 2.) 3 h; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 60, # 16 p. 5295 - 5298
反应条件
aluminium trichloride; nitrogen trichloride; 1-bromo-1,1-dimethylethane
参考文献
Tetrahedron, , vol. 23, p. 3977 - 3984
反应条件
hydrogen; Lindlar's catalyst in ethanol
参考文献
Chemistry - A European Journal, , vol. 13, # 33 p. 9207 - 9215
反应条件
T=-78 - 0°C; 2 h; 5.0 equival. MeCeCl2;
参考文献
Calderwood, David J.; Davies, Roy V.; Rafferty, Paul; Twigger, Helen L.; Whelan, Helen M.
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1241 - 1244
反应条件
1: 1.) SOCl2; 2.) HCl gas, 3.) ZnCl2 / 1.) pyridine 2: 8N hydrochloric acid / H2O / 70-80 deg C, 0.5 h; reflux, 0.5 h View Scheme
参考文献
Agricultural and Biological Chemistry, , vol. 49, # 12 p. 3563 - 3568
反应条件
1: tetrahydrofuran 2: 1.) SOCl2; 2.) HCl gas, 3.) ZnCl2 / 1.) pyridine 3: 8N hydrochloric acid / H2O / 70-80 deg C, 0.5 h; reflux, 0.5 h View Scheme
参考文献
Agricultural and Biological Chemistry, , vol. 49, # 12 p. 3563 - 3568
