甲基3-[4-(烯丙氧基)苯基]丙酸酯合成路线 (共 3 条)
反应条件
tetra-(n-butyl)ammonium iodide; potassium carbonate in N,N-dimethyl-formamide
T=20°C; 18 h; Inert atmosphere;
参考文献
ADELAIDE RESEARCH and INNOVATION PTY LTD; ABELL, Andrew David; CHUA, Krystle
Patent: WO2014/75146 A1, 2014 ;
Location in patent: Paragraph 00212; 00213 ;
反应条件
1: 98 percent / H2SO4; H2 / Pd/C
2: 74 percent / NaH; Bu4NI / tetrahydrofuran
View Scheme
参考文献
Bressy, Cyril; Piva, Olivier
Synlett, 2003 , # 1 p. 87 - 90
反应条件
water; lithium hydroxide hydrate in tetrahydrofuran
T=40°C; 3.5 h;
参考文献
ADELAIDE RESEARCH and INNOVATION PTY LTD; ABELL, Andrew David; CHUA, Krystle
Patent: WO2014/75146 A1, 2014 ;
Location in patent: Paragraph 00214; 00215 ;