(9ci)-N-[(E)-(甲氧基亚氨基)甲基]-N,N-二甲基脲合成路线 （共 3 条）
反应条件
triethylamine in dichloromethane
T=20°C; 12 h;
参考文献
Diaz, David D.; Finn
Chemistry - A European Journal, 2004 , vol. 10, # 1 p. 303 - 309
反应条件
1: 1,3-dimethyl-1-methoxyiminomethylurea With n-butyllithium in tetrahydrofuran; hexane
T=-78 - 0°C; 0.333333 h;
2: 4-bromophenyl isocyanate in tetrahydrofuran; hexane
T=-78 - 20°C; 21.5 h;
参考文献
Diaz, David D.; Finn
Organic Letters, 2004 , vol. 6, # 1 p. 43 - 46
反应条件
1: 1,3-dimethyl-1-methoxyiminomethylurea With n-butyllithium in tetrahydrofuran; hexane
T=-78 - 0°C; 0.333333 h;
2: phenyl isocyanate in tetrahydrofuran; hexane
T=-78 - 20°C; 21.5 h;
参考文献
Diaz, David D.; Finn
Organic Letters, 2004 , vol. 6, # 1 p. 43 - 46
