3,5,6-三氯吡啶-2-醇合成路线 （共 25 条）
反应条件
potassium hydroxide in ethanol 4 h; Heating;
参考文献
Watanabe, Eiki; Hoshino, Ryoko; Kanzaki, Yukiko; Tokumoto, Hiroshi; Kubo, Hiroaki; Nakazawa, Hiroyuki
Journal of agricultural and food chemistry, 2002 , vol. 50, # 13 p. 3637 - 3646
反应条件
hydrogenchloride; Copper(I)chloride in sulfolane
反应条件
hydrogenchloride; sodium carbonate in sulfolane
反应条件
1: With copper(l) chloride T=120 - 150°C; P=1140.08 - 4560.31 Torr; 6 h; 2: With water; sodium hydroxide T=30 - 150°C; P=1520.1 Torr;
参考文献
Fakhraian; Moghimi; Bazaz; Hadj-Ghanbary; Sadeghi
Organic Process Research and Development, 2003 , vol. 7, # 3 p. 329 - 333
反应条件
potassium hydroxide in tert-butyl alcohol 10 h; Heating;
参考文献
Raju, B. China; Neelakantan, Parvathi; Bhalerao
Synthetic Communications, 2004 , vol. 34, # 16 p. 2903 - 2909
反应条件
hydrogenchloride; water; C15H21INO9PolSi T=25°C; pH=7.4; 0.00833333 h; Rate constant;
参考文献
WO2009/55128 A2, ;
Page/Page column 48-52 ;
反应条件
Copper(I)chloride in acetonitrile
反应条件
1: 97 percent / HCl / ethyl acetate / 2 h / 25 °C / 5171.5 Torr 2: 100 percent / aq. NaOH / 1,2-dichloro-ethane / 20 h / 25 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 59, # 22 p. 6783 - 6785
反应条件
copper(l) chloride T=120 - 150°C; P=1140.08 - 4560.31 Torr; 6 h; Overall yield = 182 g;
参考文献
Organic Process Research and Development, , vol. 7, # 3 p. 329 - 333
反应条件
copper(l) chloride T=150°C; P=4560.31 Torr; 5 h;
参考文献
Organic Process Research and Development, , vol. 7, # 3 p. 329 - 333
