1: With sodium hydroxide in water 4 h; Heating / reflux; 2: With hydrogenchloride in water T=20°C;
参考文献
Hormann, Robert Eugene; Potter, David W.; Chortyk, Orestes; Tice, Colin M.; Carlson, Glenn Richard; Meyer, Andrew; Opie, Thomas R.
Patent: US2006/20146 A1, 2006 ;
Location in patent: Page/Page column 30 ;
1: 3-(fluorophenyloxy)triisopropylsilane With N,N,N',N'',N''-pentamethyldiethylenetriamine; sec.-butyllithium in tetrahydrofuran T=-75°C; 2 h; 2: carbon dioxide in tetrahydrofuran
参考文献
European Journal of Organic Chemistry, , # 10 p. 2116 - 2123
1: 3-(methoxymethoxy)-2-(trimethylsilyl)fluorobenzene With n-butyllithium; potassium tert-butylate in tetrahydrofuran; hexane T=-75°C; 2 h; 2: carbon dioxide in tetrahydrofuran; hexane 3: With hydrogenchloride in water T=25°C; 6 h;
参考文献
European Journal of Organic Chemistry, , # 10 p. 2116 - 2123
