2-乙酰基-3,5-二甲氧基苯乙酸甲酯合成路线 （共 5 条）
反应条件
1: NaOMe / methanol View Scheme
参考文献
Bycroft,B.W.; Roberts,J.C.
Journal of the Chemical Society, 1963 , p. 4868 - 4872
反应条件
perchloric acid; acetic acid in water
T=35°C; Friedel-Crafts Acylation; 0.0833333 h;
参考文献
Beekman, Andrew Michael; Barrow, Russell Allan
Journal of Natural Products, 2013 , vol. 76, # 11 p. 2054 - 2059
反应条件
AlCl3, aluminium chloride in dichloromethane
T=0 - 20°C; Friedel-Crafts Acylation; 1.83333 h;
参考文献
Meier, Robin; Strych, Sebastian; Trauner, Dirk
Organic Letters, 2014 , vol. 16, # 10 p. 2634 - 2637
反应条件
cesium fluoride in acetonitrile
T=80°C; Inert atmosphere;
参考文献
Allan, Kevin M.; Hong, Boram D.; Stoltz, Brian M.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 23 p. 4960 - 4964
反应条件
sodium hydride in N,N-dimethyl-formamide; mineral oil
T=20°C; 1 h; Inert atmosphere;
参考文献
Pepper, Henry P.; George, Jonathan H.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 46 p. 12170 - 12173
Angew. Chem., 2013 , vol. 125, # 46 p. 12392 - 12395,4
