3,5-二甲氧基苯乙酸甲酯合成路线 (共 20 条)
反应条件
sulfuric acid 4 h; Heating;
参考文献
Saeed, Aamer; Rama, Nasim H.; Arfan
Journal of Heterocyclic Chemistry, 2003 , vol. 40, # 3 p. 519 - 522
反应条件
lead(IV) tetraacetate in dichloromethane T=20°C; 0.666667 h;
参考文献
Beekman, Andrew Michael; Barrow, Russell Allan
Journal of Natural Products, 2013 , vol. 76, # 11 p. 2054 - 2059
反应条件
in acetone 12 h; Heating;
参考文献
Liang, Qiren; Zhang, Jiyong; Quan, Weiguo; Sun, Yongquan; She, Xuegong; Pan, Xinfu
Journal of Organic Chemistry, 2007 , vol. 72, # 7 p. 2694 - 2697
反应条件
1: 78 percent / potassium iodide; formic acid / chloro(1,5-cyclooctadiene)rhodium(I) dimer / 24 h / 60 °C / 760 Torr 2: 100 percent / conc. sulfuric acid / 4 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 40, # 3 p. 519 - 522
反应条件
pyridine; thionyl chloride; silver(l) oxide 1. benzene, 1 h, reflux 2. ethyl ether, r.t., 1 h 3. reflux, 1 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 56, # 14 p. 4499 - 4508
反应条件
1: 1) SOCl2 View Scheme
参考文献
Tetrahedron Letters, , vol. 32, # 23 p. 2663 - 2666
反应条件
1: (i) LiAlH4, (ii) PBr3 2: ethanol 3: (i) NaOH, MeOH, (ii) /BRN= 102415/ View Scheme
参考文献
Tetrahedron, , vol. 18, p. 1519 - 1526
反应条件
in methanol; diethyl ether; benzene 0.5 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 17, # 12 p. 3281 - 3286
参考文献
Tetrahedron Letters, , vol. 32, # 23 p. 2663 - 2666
反应条件
(i) NaOH, MeOH, (ii) /BRN= 102415/; Multistep reaction;
参考文献
Tetrahedron, , vol. 18, p. 1519 - 1526