tris(dimethylamino)-sulphonium difluorotrimethylsilicate in tetrahydrofuran T=20°C;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 7.2 p. 1539
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 7 p. 1693 - 1694
Karpov, V. M.; Panteleev, I. V.; Platonov, V. E.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, p. 1932 - 1938
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, p. 2183 - 2191
water; SbF5; silica gel T=75°C; 4 h; also in the absence of SiO2; other temp. and time; multistep 1.) 75 deg C, 4 h; Product distribution;
参考文献
Karpov, V. M.; Panteleev, I. V.; Platonov, V. E.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, p. 1932 - 1938
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, p. 2183 - 2191
1: 1.) SbF5, SiO2, 2.) H2O / 1.) 75 deg C, 4 h 2: 7.09 g / SOCl2, DMF / 3 h / 80 - 110 °C 3: 3.14 g / KF / 16 h / 200 °C View Scheme
参考文献
Karpov, V. M.; Panteleev, I. V.; Platonov, V. E.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, p. 1932 - 1938
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, p. 2183 - 2191
